This program of research was directed at developing techniques for the screening of the presence of controlled substances from air samples. This dataset contains raw data and processed data in relation to the analysis of air samples for controlled substances. This dataset cannot be openly published due to ethics conditions. To discuss this research, please contact Val Spikmans V.Spikmans@westernsydney.edu.au ORCID 0000-0001-5648-8330